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NMR-on-a-Chip Devised

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GAITHERSBURG, Md., Feb. 20, 2008 -- A supersensitive minisensor can detect nuclear magnetic resonance (NMR) in tiny liquid samples flowing through a novel microchip. The prototype device, which combines an atomic magnetometer with a fluid channel, could be used to rapidly screen for new drugs, or to track fluid or gas flow for industrial processes and oil exploration.

The "nuclear magnetic resonance on a chip" device was developed at the National Institute of Standards and Technology (NIST) in collaboration with the University of California at Berkeley. In experiments, it was able to detect magnetic signals from atomic nuclei in tap water flowing through a tiny fluid channel on a custom silicon chip.

The Berkeley group recently co-developed this "remote NMR" technique for tracking small volumes of fluid or gas flow inside soft materials such as biological tissue or porous rock for industrial and oil exploration applications. The chip could also be used in NMR spectroscopy, a widely used technique for determining physical, chemical, electronic and structural information about molecules. NMR signals are equivalent to those detected in MRI (magnetic resonance imaging) systems.
NMRChip.jpg
Prototype microchip device combines the National Institute of Standards and Technology's miniature atomic magnetometer with a fluid channel for studying tiny samples. (Image courtesy NIST)
Berkeley scientists selected the NIST sensor, a type of atomic magnetometer and a spinoff of its tiny atomic clocks, for the chip device because of its small size and high sensitivity, which make it possible to detect weak magnetic resonance signals from a small sample of atoms in the adjacent microchannel. The minisensor has also been shown to have biomedical imaging applications.

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Detection is most efficient when the sensor and sample are about the same size and located close together, said Micah Ledbetter, lead author of a paper on the research, making a small sensor crucial for working with small samples.

Its small size and extreme sensitivity make the NIST sensor ideal for the microchip device, in contrast to SQUIDs (superconducting quantum interference devices) that require bulky equipment for cooling to cryogenic temperatures or conventional copper coils that need much higher magnetic fields (typically generated by large, superconducting magnets) like those in traditional MRI, the researchers said. A joint university/NIST patent application is being filed for the device.

The principal investigator for the study, published this month in the Proceedings of the National Academy of Sciences (PNAS), is Alexander Pines, a leading authority on NMR. The research was supported by the Office of Naval Research, US Department of Energy, a California Space Institute (CalSpace) minigrant and DARPA.

For more information, visit: www.nist.gov

Published: February 2008
Glossary
atomic clock
An atomic clock is a highly precise timekeeping device that uses the vibrations or oscillations of atoms as a reference for measuring time. The most common type of atomic clock uses the vibrations of atoms, typically cesium or rubidium atoms, to define the length of a second. The principle behind atomic clocks is based on the fundamental properties of atoms, which oscillate at extremely stable and predictable frequencies. The primary concept employed in atomic clocks is the phenomenon of...
magnetometer
A magnetometer is a scientific instrument used to measure the strength and/or direction of a magnetic field. It can detect and quantify the intensity of magnetic fields in its vicinity. Magnetometers are employed in various applications, including geophysics, navigation, archaeology, and space exploration. There are different types of magnetometers, each with its own operating principles. Common types include fluxgate magnetometers, proton precession magnetometers, and magneto-resistive...
nano
An SI prefix meaning one billionth (10-9). Nano can also be used to indicate the study of atoms, molecules and other structures and particles on the nanometer scale. Nano-optics (also referred to as nanophotonics), for example, is the study of how light and light-matter interactions behave on the nanometer scale. See nanophotonics.
nuclear magnetic resonance
A phenomenon, exploited for medical imaging, in which the nuclei of material placed in a strong magnetic field will absorb radio waves supplied by a transmitter at particular frequencies. The energy of the radio-frequency photons is used to promote the nucleus from a low-energy state, in which the nuclear spin is aligned parallel to the strong magnetic field, to a higher-energy state in which the spin is opposed to the field. When the source of the radio waves is turned off, many nuclei will...
photonics
The technology of generating and harnessing light and other forms of radiant energy whose quantum unit is the photon. The science includes light emission, transmission, deflection, amplification and detection by optical components and instruments, lasers and other light sources, fiber optics, electro-optical instrumentation, related hardware and electronics, and sophisticated systems. The range of applications of photonics extends from energy generation to detection to communications and...
atomic clockatomic nucleiBasic ScienceBerkeleybiomedicalbiomedical imagingBiophotonicsindustrialmagnetometermicrochipminisensorMRInanoNews & FeaturesNISTNMRnuclear magnetic resonancephotonicsPNASSensors & DetectorsspectroscopySQUIDssuperconductingsupersensitive

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